facile and economic method for preparation of nano-colloidal silica with controlled size and stability
نویسندگان
چکیده
this study is focused on synthesis of nano-colloidal silica via alkaline water glass solution. sodium ions of water glass were removed by cation exchanging in a resin column to obtain the silicic acid which was titrated to the solution of sodium silicate. concentration of the colloidal silica and ph value of the solutions were controlled using different concentrations of alkaline sodium silicate and silicic acid solutions in constant temperature and titration rate. the synthesized colloidal silica was characterized by dynamic light scattering (dls), scanning electron microscopy (sem), x-ray powder diffraction (xrd), accelerated surface area and porosimetry analyzer (asap) and gravimetric method. the results showed that the average particle size of colloids and their stability were also influenced by various important factors such as ph, temperature, concentrations of alkaline sodium silicate and silicic acid solutions. the results showed that the synthesized nano-colloidal silica suspensions in concentration up to 25 wt.% of sio2 with average particle sizes in range of 23 to100 nm are stable more than one year. also, surface area and pore volume of the prepared spherical colloidal silica particles were160 m2/g and 0.27 cm2/g, respectively.
منابع مشابه
Facile and economic method for preparation of nano-colloidal Silica with controlled size and stability
This study is focused on synthesis of nano-colloidal silica via alkaline water glass solution. Sodium ions of water glass were removed by cation exchanging in a resin column to obtain the silicic acid which was titrated to the solution of sodium silicate. Concentration of the colloidal silica and pH value of the solutions were controlled using different concentrations of alkaline sodium silicat...
متن کاملFacile and economic method for preparation of nano-colloidal Silica with controlled size and stability
This study is focused on synthesis of nano-colloidal silica via alkaline water glass solution. Sodium ions of water glass were removed by cation exchanging in a resin column to obtain the silicic acid which was titrated to the solution of sodium silicate. Concentration of the colloidal silica and pH value of the solutions were controlled using different concentrations of alkaline sodium silicat...
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Preparation and Characterization of Colloidal Silica in Alkaline and Constant Range of pH
In this study, alkaline colloidal silica was prepared by titration of an alkaline solution such as sodium silicate with silicic acid in constant range of pH .This constant range of pH was achieved by using concentrated soduim silicate solutions as pH adjusting solutions during titration.The sodium silicate solutions having a variety of...
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عنوان ژورنال:
international journal of nano dimensionجلد ۵، شماره ۲، صفحات ۱۷۷-۱۸۵
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